Benzyl Alcohol → HCID 68120100, compound

HRID 2398574Notes

Reaction equation

HRID 2398574 reaction equation
[N:1]([C:4]1[CH:9]=[CH:8][C:7]([CH3:10])=[C:6]([N:11]2[C:15](=[O:16])[C:14]3=[CH:17][C:18]([Cl:21])=[CH:19][CH:20]=[C:13]3[C:12]2=[O:22])[CH:5]=1)=[C:2]=[O:3].[CH2:23]([OH:30])[C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1>>[CH2:23]([O:30][C:2]([NH:1][C:4]1[CH:9]=[CH:8][C:7]([CH3:10])=[C:6]([N:11]2[C:15](=[O:16])[C:14]3=[CH:17][C:18]([Cl:21])=[CH:19][CH:20]=[C:13]3[C:12]2=[O:22])[CH:5]=1)=[O:3])[C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1

Participants

3

Reactant 2

HCID 244Benzyl AlcoholHCID 86734767HCID 86734767, compound

Product 1

HCID 68120100HCID 68120100, compound

Procedure

The starting material is prepared as follows: The mixture of 0.5 g of N-(4-isocyanato-o-tolyl)-4-chlorophthalimide and 5ml of benzyl alcohol is heated to 120° under nitrogen for 6 hours and evaporated, to yield the N-(4-benzyloxycarbonylamino-o-tolyl)-4-chlorophthalimide.

Workup

  1. customThe starting material is prepared
  2. temperatureis heated to 120° under nitrogen for 6 hours
  3. customevaporated

Sources & evidence

ORD record
ord-e8821164fbb448f5912b559de837faa1
Source dataset
uspto-grants-1977_05
Patent number
US04025505

Reaction notes

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