Thionyl Chloride → HCID 20369306, compound

HRID 2398606Notes

Reaction equation

HRID 2398606 reaction equation
[ClH:1].[C:2]([CH2:5][CH2:6][C:7]([OH:9])=O)(=[NH:4])[NH2:3].S(Cl)([Cl:12])=O>>[ClH:12].[C:2]([CH2:5][CH2:6][C:7]([Cl:1])=[O:9])(=[NH:4])[NH2:3]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 86733246HCID 86733246, compound

Product 1

HCID 20369306HCID 20369306, compound

Procedure

A solution of 1.52 g. (0.01 mole) of 3-amidinopropionic acid hydrochloride in 18 ml. of thionyl chloride is allowed to stir at room temperature overnight. The excess solvent-reactant is then removed under reduced pressure and the product is isolated as a yellow gum, which crystallizes on standing, 1.5 g.

Workup

  1. customThe excess solvent-reactant is then removed under reduced pressure
  2. customthe product is isolated as a yellow gum, which
  3. customcrystallizes

Sources & evidence

ORD record
ord-e6bd2eb3c1734b81abb0672909b6385d
Source dataset
uspto-grants-1977_05
Patent number
US04025504

Reaction notes

Loading…