HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12452842, compound → 3-Furancarboxylic acid, 2-methyl-5-pentyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12452842 | HCID 12452842 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | 3-Furancarboxylic acid, 2-methyl-5-pentyl- | HCID 21433407 | — |
Reaction Steps
Saponification of the ester was accomplished by refluxing 12 hours in 10 ml of 25% aqueous sodium hydroxide and 5 ml of ethanol. Acidification precipitated the crude acid, which was purified by sublimation to give 2-methyl-5-pentyl-3-furoic acid, mp 47°-48° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04025537 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-76efe4b2f3c344b4992f2f158a92143c |
| Source note | uspto-grants-1977_05 |