HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 12452844, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 53678912 | HCID 53678912 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 12452844 | HCID 12452844 | 63% |
Reaction Steps
A mixture of 2.64 g (8.15 mmole) ethyl 2-acetyl-2-hexadecenoate and 1.45 g (8.15 mmole) N-bromosuccinimide in 25 ml of carbon tetrachloride was heated at reflux for 12 hours. After cooling, the succinimide was removed by filtration and the solution concentrated in vacuo. Distillation of the crude product gave 1.65 g (63%) of ethyl 5-dodecyl-2-methyl-3-furoate, bp 160°-163° C. (0.4 mm).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04025537 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-27403d0513cf401a84db85a6eff3e31a |
| Source note | uspto-grants-1977_05 |