HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12452844, compound → HCID 21433412, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12452844 | HCID 12452844 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 21433412 | HCID 21433412 | — |
Reaction Steps
Saponification of 0.5 g of the ester was accomplished by refluxing 12 hours in 10 ml of 25% aqueous sodium hydroxide and 5 ml of ethanol. Acidification of the mixture precipitated the crude acid, which was purified by sublimation to give 5-dodecyl-2-methyl-3-furoic acid, mp 70°-73° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04025537 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-adb31d65afb94384a4cb390b4674e7e4 |
| Source note | uspto-grants-1977_05 |