Methanol, 1,1'-oxybis-, 1,1'-diacetate → HCID 9856089, compound

Participants

Reaction Steps

Using the procedure of Example 2, acetyl methanesulfonate and tetroxane, in a molar ratio of 2:1, were reacted for 18-24 hours at 90° C. and 0.5 mm. pressure allowing the bis(acetoxymethyl) ether to distill. The residual oil was recrystallized from a small volume of dry tetrahydrofuran to give a 67% yield of CH3SO3CH2OCH2OSO2CH3.

Provenance & Evidence