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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2398671Generated: October 31, 2026

methylsulfonyl acetate → HCID 9856089, compound

https://huagongshe.com/reaction/2398671

Reaction equation

Participants

RoleNameHCIDCharge
Reactantmethylsulfonyl acetateHCID 292469—
ReactantHCID 131710792HCID 131710792—
ProductHCID 9856089HCID 985608941.8%

Reaction Conditions

Temperature25 °C

Reaction Steps

A mixture of 12.7 g of acetyl methanesulfonate and 9.15 g of trioxymethylene diacetate was prepared at 0° C. and then stirred at 25° C. for 20 hours. Distillation at 10μ produced 4.5 g of CH3SO3CH2OCH2OSO2CH3, b.p. 110°-115° C. (pot temp.); m.p. 57°-59° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04025542
Source datasetuspto-grants-1977_05
ORD IDord-2a9a3e7149dc4cf9b0acf80d015bacab
Source noteuspto-grants-1977_05