HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stearic Acid → Monostearin
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stearic Acid | HCID 5281 | — |
| Reactant | Glycidol | HCID 11164 | — |
| Catalyst | Sodium Hydroxide | HCID 14798 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Monostearin | HCID 24699 | 86.1% |
Reaction Steps
0.4 mole of stearic acid were heated to boiling (about 113° C.) under reflux with 280 grams of toluene and 0.29 gram of NaOH (water free) and, in the course of 20 minutes, 31.2 grams of glycidol dropped in. After a further 5 hours at this temperature, the glycidol was 99% reacted and the reaction ended. After working as in Example 1, there were obtained 123.5 grams (86%) of monostearin having the following properties:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04025540 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-02a35e47b46641f4a943d864ec83ee1a |
| Source note | uspto-grants-1977_05 |