HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonamide, 3-amino- → HCID 178467268, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonamide, 3-amino- | HCID 7377 | — |
| Reactant | 3,5-Diacetyl-2,6-dihydroxy-4h-pyran-4-one | HCID 135465969 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178467268 | HCID 178467268 | — |
Reaction Steps
To a hot solution of 2.12 g. (0.01 mol) of 3,5-diacetyl-4,6-dihydroxy-2H-pyran-2-one in 40 ml. of methanol is added 1.72 g. (0.01 mol) of m-sulfamylaniline and the mixture is refluxed for one hour. The solid is filtered from the reaction mixture to obtain 5-acetyl-4-hydroxy-3-[1-(3-sulfamylphenylamino)ethylidene]-2H-pyran-2,6(3H)-dione, m.p. 237° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04025614 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-72bbf76f3b0644eb9cbfb30b16c85a1c |
| Source note | uspto-grants-1977_05 |