2-Aminobenzimidazole → HCID 22797768, compound

Participants

Reaction Conditions

Reaction Steps

To 10 ml of anhydrous xylene were added 390 mg (1 mmol) of 2,3,4,6-tetra-O-acetyl-D-glucopyranosyl isothiocyanate and 135 mg (1 mmol) of 2-aminobenzimidazole (MW 133) and the mixture was heated at 100° C. for 1 hour and allowed to cool to room temperature. Crystals formed were filtered off and recrystallized from methanol to give colourless needles melting between 162° and 165° C. (uncorrected). Yield: 245 mg (47%).

Provenance & Evidence