Benzo(d)thiazol-2-amine → HCID 22797769, compound

Participants

Reaction Conditions

Reaction Steps

To 10 ml of anhydrous xylene were added 390 mg (1 mmol) of 2,3,4,6-tetra-O-acetyl-D-glucopyranosyl isothiocyanate and 150 mg (1 mmol) of 2-aminobenzothiazole (MW 150) and the mixture was heated at 110° C. for 40 minutes and allowed to cool to room temperature. Crystals formed were filtered off and recrystallized from methanol to give colourless needles melting between 179° and 181° C. (uncorrected). Yield: 230 mg (42%).

Provenance & Evidence