Dinitrofluorobenzene → 1-(2-Acetamidoethyl)-5-(2,4-dinitrophenylthio)tetrazole

Participants

Reaction Steps

A solution of 9.3 g. (0.050 mol.) of 2,4-dinitrofluorobenzene in 50 ml. of acetone was added to a solution of 9.35 g. (0.050 mol.) of 1-(2-acetamidoethyl)tetrazole-5-thiol and 6.85 ml. (0.050 mol.) of triethylamine in 100 ml. of acetone and the reaction mixture was stirred for 1 hour. The solid was collected and recrystallized from acetonitrile to give 1-(2-acetamidoethyl)-5-(2,4-dinitrophenylthio)-tetrazole, m.p. 197°-198°.

Provenance & Evidence