Sodium Hydroxide → HCID 23671259, compound

HRID 2398818Notes

Reaction equation

HRID 2398818 reaction equation
[CH2:1]([CH:4]([CH2:10][CH2:11][CH3:12])[CH2:5][CH2:6][C:7]([OH:9])=[O:8])[CH2:2][CH3:3].[OH-].[Na+:14]>O>[CH2:10]([CH:4]([CH2:1][CH2:2][CH3:3])[CH2:5][CH2:6][C:7]([O-:9])=[O:8])[CH2:11][CH3:12].[Na+:14]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 18623020HCID 18623020, compound

Product 1

HCID 23671259HCID 23671259, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

In a flask, 17.2 g (0.1 mol) of 4-n-propyl-heptanoic acid, prepared as described in the above Example 2, were dissolved in a sufficient volume of water. After that 4 g (0.1 mol) of a sodium hydroxide solution in water were added and the mixture was evaporated to dryness. The residue so obtained was rinsed with ethyl ether and maintained in a dessicator under vacuum.

Workup

  1. customthe mixture was evaporated to dryness
  2. customThe residue so obtained
  3. washwas rinsed with ethyl ether
  4. temperaturemaintained in a dessicator under vacuum

Sources & evidence

ORD record
ord-dd7a4ab098b24895a137606a980adb0a
Source dataset
uspto-grants-1977_05
Patent number
US04025649

Reaction notes

Loading…