HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl isocyanate → HCID 20543608, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl isocyanate | HCID 62412 | — |
| Reactant | 1-(2,6-Xylyl)thiourea | HCID 853911 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 20543608 | HCID 20543608 | — |
Reaction Steps
To a mixture of 8.8 g. (0.05 mole) of 1-(2,6-dimethylphenyl)thiourea and 10 ml. of xylene is added 5 g. of t-butylisocyanate (0.05 mole) and the mixture is refluxed for 2 hours. The reaction product is cooled, triturated with heptane and filtered. Recrystallization from 1:1 isopropanol/water results in 1-(2,6-dimethylphenyl)-3-(t-butylcarbamyl)thiourea.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04025652 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-84928cef24dc45059285e946fac1761e |
| Source note | uspto-grants-1977_05 |