HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → 2,6-Dimethylpiperidine-1-carbonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | Nanofin | HCID 68843 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 2,6-Dimethylpiperidine-1-carbonyl chloride | HCID 19070661 | — |
Reaction Steps
To a solution of 50 g. of 2,6-dimethylpiperidine in 300 ml. of benzene is added 60 g. of phosgene and the mixture is refluxed for 3 hours. The solid which had separated was filtered and the filtrate was concentrated and distilled under vacuum to obtain 2,6-dimethylpiperidinoyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04025652 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-cbdfda2681194d29a5c7b8a5620b4153 |
| Source note | uspto-grants-1977_05 |