HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylcarbodiimide → HCID 21433919, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | 1-Piperidinepropanoic acid | HCID 117782 | — |
| Reactant | HCID 21433908 | HCID 21433908 | — |
| Product | HCID 21433919 | HCID 21433919 | — |
Reaction Steps
Following the procedure similar to that described in Example 8 hereinabove, 1,2-dihydro-9-hydroxy-7-methyl-4-oxo-4H-thieno[2,3-c][1]benzopyran is reacted with methyl magnesium bromide to give 1,2-dihydro-9-hydroxy-4,4,7-trimethyl-4H-thieno-[2,3-c][1]benzopyran. The benzopyran is then reacted with β-piperidinopropionic acid and dicyclohexylcarbodiimide to yield the desired ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04025630 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-5dc1dd4b71b7406f947d9e8191820d85 |
| Source note | uspto-grants-1977_05 |