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HRID2398949

反应详情

EQUATION

反应方程式

HRID 2398949 的结构方程式

REACTANTS

反应物

2
结构：[Na+].[OH-]
HCID14798

Sodium Hydroxide

HNaO

结构：O=C(O)COc1ccc(NC(=O)C=Cc2ccc(O)cc2)cc1
HCID54078252

未命名化合物

PRODUCTS

生成物

1
结构：O=C([O-])COc1ccc(NC(=O)C=Cc2ccc(O)cc2)cc1.[Na+]
HCID68119543

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOCC
溶剂HCID3283

Diethyl Ether

C4H10O

PROCEDURE

实验过程

156 Milligrams of 4-(4'-hydroxycinnamoylamino)phenoxyacetic acid were dissolved in an alcohol and an equivalent amount of sodium hydroxide was added to the solution. The solution was warmed for 30 minutes. After cooling, ether was added to the solution and the precipitated crystals were collected by filtration to obtain sodium 4-(4'-hydroxycinnamoylamino)phenoxyacetate.

WORKUP

后处理

  1. temperatureThe solution was warmed for 30 minutes
  2. temperatureAfter cooling
  3. filtrationthe precipitated crystals were collected by filtration