Sodium Hydroxide → HCID 68119543, compound

HRID 2398949Notes

Reaction equation

HRID 2398949 reaction equation
[OH:1][C:2]1[CH:23]=[CH:22][C:5]([CH:6]=[CH:7][C:8]([NH:10][C:11]2[CH:21]=[CH:20][C:14]([O:15][CH2:16][C:17]([OH:19])=[O:18])=[CH:13][CH:12]=2)=[O:9])=[CH:4][CH:3]=1.[OH-].[Na+:25]>CCOCC>[OH:1][C:2]1[CH:3]=[CH:4][C:5]([CH:6]=[CH:7][C:8]([NH:10][C:11]2[CH:21]=[CH:20][C:14]([O:15][CH2:16][C:17]([O-:19])=[O:18])=[CH:13][CH:12]=2)=[O:9])=[CH:22][CH:23]=1.[Na+:25]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 54078252HCID 54078252, compound

Product 1

HCID 68119543HCID 68119543, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

156 Milligrams of 4-(4'-hydroxycinnamoylamino)phenoxyacetic acid were dissolved in an alcohol and an equivalent amount of sodium hydroxide was added to the solution. The solution was warmed for 30 minutes. After cooling, ether was added to the solution and the precipitated crystals were collected by filtration to obtain sodium 4-(4'-hydroxycinnamoylamino)phenoxyacetate.

Workup

  1. temperatureThe solution was warmed for 30 minutes
  2. temperatureAfter cooling
  3. filtrationthe precipitated crystals were collected by filtration

Sources & evidence

ORD record
ord-1a8dcc8a741040afaebb9ca25ef7548b
Source dataset
uspto-grants-1977_05
Patent number
US04026896

Reaction notes

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