Sodium Hydroxide → HCID 68119810, compound

HRID 2398951Notes

Reaction equation

HRID 2398951 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:21]=[CH:22][C:23]=1[O:24][CH2:25][CH2:26][CH3:27])[CH:6]=[CH:7][C:8]([NH:10][C:11]1[CH:16]=[CH:15][C:14]([CH2:17][C:18]([OH:20])=[O:19])=[CH:13][CH:12]=1)=[O:9].[OH-].[Na+:29]>CCOCC>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:21]=[CH:22][C:23]=1[O:24][CH2:25][CH2:26][CH3:27])[CH:6]=[CH:7][C:8]([NH:10][C:11]1[CH:16]=[CH:15][C:14]([CH2:17][C:18]([O-:20])=[O:19])=[CH:13][CH:12]=1)=[O:9].[Na+:29]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 53878665HCID 53878665, compound

Product 1

HCID 68119810HCID 68119810, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

184 Milligrams of 4-(3'-methoxy-4'-propoxycinnamoylamino)phenylacetic acid were dissolved in an alcohol and an equivalent amount of sodium hydroxide was added to the solution. The solution was warmed for 30 minutes. After cooling, ether was added to the solution and the precipitated crystals were collected by filtration to obtain sodium 4-(3'-methoxy-4'-propoxycinnamoylamino)phenylacetate.

Workup

  1. temperatureThe solution was warmed for 30 minutes
  2. temperatureAfter cooling
  3. filtrationthe precipitated crystals were collected by filtration

Sources & evidence

ORD record
ord-9e3303a0f38c4fdea0ec69588e75fcb4
Source dataset
uspto-grants-1977_05
Patent number
US04026896

Reaction notes

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