HCID 1332826, compound → HCID 21432597, compound

HRID 2399036Notes

Reaction equation

HRID 2399036 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([CH:15]=[CH:16][C:17]=1Cl)[C:7]([C:9]1[CH:14]=[CH:13][N:12]=[CH:11][CH:10]=1)=[O:8])([O-:3])=[O:2].C[N:20](C)C=O.CC(O)C>>[N+:1]([C:4]1[CH:5]=[C:6]([CH:15]=[CH:16][C:17]=1[NH2:20])[C:7]([C:9]1[CH:14]=[CH:13][N:12]=[CH:11][CH:10]=1)=[O:8])([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 1332826HCID 1332826, compoundHCID 20197112Isopropanol dimethylformamide

Product 1

HCID 21432597HCID 21432597, compound

Procedure

The procedure of Example 24 was followed except 4-(3-nitro-4-chlorobenzoyl)pyridine was used in place of 3-(3-nitro-4-chlorobenzoyl)pyridine. The product was orange prisms, mp. 294° -295° C. (dimethylformamide-2-propanol).

Sources & evidence

ORD record
ord-c59aa92294244a04877200ffab0f8376
Source dataset
uspto-grants-1977_05
Patent number
US04026936

Reaction notes

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