HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxy-1,3-butadiene → (+/-)-6-Benzoyloxy-2-methoxy-2,7,8-trimethylchroman
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxy-1,3-butadiene | HCID 99338 | — |
| Reactant | 4-Benzoyloxy-2,3-dimethylphenol | HCID 15870860 | — |
| Product | (+/-)-6-Benzoyloxy-2-methoxy-2,7,8-trimethylchroman | HCID 21432306 | — |
Reaction Steps
By the manner of Example 45, 4-benzoyloxy-2,3-dimethylphenol was reacted with 2-methoxybutadiene to give (±)-6-benzoyloxy-2-methoxy-2,7,8-trimethylchroman as a white powder, m.p. 101.5°-102.5°, from ether-30°-60° petroleum ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04026907 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-906efe7f349849f8b209c5ca83050f02 |
| Source note | uspto-grants-1977_05 |