Ethanol → 11-Mercaptoundecanol

HRID 239910Notes

Reaction equation

HRID 239910 reaction equation
[C:1]([OH:20])(=O)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11]CCCCCCC.[SH:21]C(O)CCCCCCCCCC.C(O)C>C(Cl)(Cl)Cl>[SH:21][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][CH2:1][OH:20]

Participants

5

Reactant 3

HCID 702EthanolHCID 445639Oleic AcidHCID 22149515HCID 22149515, compound

Product 1

HCID 26182411-Mercaptoundecanol

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent2×

Procedure

Five (5) mg of the oleic acid-stabilized CdSe quantum dots and 50 mg of 1-mercapto-1-undecanol were mixed with 5 ml of chloroform and 5 ml of ethanol. The mixture was then sonicated for 3 hours. Then, 40 ml of chloroform was added to the mixture to obtain a precipitate of 11-mercapto-1-undecanol capped CdSe quantum dots. The precipitate was dissolved in ethanol and dimethyl sulfoxide (“DMSO”).

Workup

  1. customThe mixture was then sonicated for 3 hours

Sources & evidence

ORD record
ord-209ad8a11ae042d6bfe69a6ab21f8162
Source dataset
uspto-grants-2014_02
Patent number
US08642991B2

Reaction notes

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