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HRID2399133

反应详情

EQUATION

反应方程式

HRID 2399133 的结构方程式

REACTANTS

反应物

2
结构：O=C(Nc1ccc2c(S(=O)(=O)[O-])cccc2c1S(=O)(=O)[O-])c1cccc([N+](=O)[O-])c1.[Na+].[Na+]
HCID88828409

未命名化合物

结构：[H][H]
HCID178418361

未命名化合物

PRODUCTS

生成物

1
结构：Nc1cccc(C(=O)Nc2ccc3c(S(=O)(=O)[O-])cccc3c2S(=O)(=O)[O-])c1.[Na+].[Na+]
HCID88828600

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Pd]
催化剂HCID23938

Palladium

Pd

结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

A mixture of 25.0 g of 2-(m-(nitrobenzamido)-1,5-naphthalenedisulfonic acid disodium salt (prepared as in Example 1), 250 ml of water and 2.0 g of 10% palladium on charcoal is hydrogenated in a Parr shaker for 31/2 hours at room temperature with an initial pressure of 42 pounds of hydrogen. During this time a total of 11.5 pounds of hydrogen is absorbed.

WORKUP

后处理

  1. custom2 hours
  2. customat room temperature
  3. customDuring this time a total of 11.5 pounds of hydrogen is absorbed