1,1-Dibromoethane → HCID 43627906, compound

HRID 2399173Notes

Reaction equation

HRID 2399173 reaction equation
[CH2:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[OH:10])[CH:2]=[CH2:3].[Br:11][CH:12](Br)[CH3:13]>>[CH2:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[O:10][CH2:13][CH2:12][Br:11])[CH:2]=[CH2:3]

Participants

3

Reactant 2

HCID 112011,1-DibromoethaneHCID 156242-Allylphenol

Product 1

HCID 43627906HCID 43627906, compoundYield 17.9%

Procedure

Using the procedure described in Example I step A and starting from 43.5 g o-allylphenol and 140 g dibromoethane, 35 g of crude product are produced which after distillation under reduced pressure give 14 g of pure compound. The latter boils at 150°-154° under 18-20 mm Hg.

Workup

  1. customare produced which
  2. distillationafter distillation under reduced pressure

Sources & evidence

ORD record
ord-c56189415cd74be98c520881a1a56fcb
Source dataset
uspto-grants-1977_05
Patent number
US04027028

Reaction notes

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