HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → HCID 19430584, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | 5-tert-amylsalicylic acid | HCID 268742 | — |
| Product | HCID 19430584 | HCID 19430584 | — |
Reaction Steps
Following the procedure of Schmitt et al., Synthesis, 1984, 758-760; and treating the resulting 2-hydroxy-5-(1,1-dimethylpropyl)benzoic acid with diazomethane gave the title compound. 1H NMR (250 MHz, CDCl3) δ10.61 (s, 1H), 7.75 (d, 1H), 7.44 (dd, 1H), 6.92 (d, 1H), 3.95 (s, 3H), 1.61 (q, 2H), 1.26 (s, 6H), 0.67 (t, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05447957 |
| Source dataset | uspto-grants-1995_09 |
| ORD ID | ord-f44abc08b31b45d3b04d675e1f275aaa |
| Source note | uspto-grants-1995_09 |