HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → HCID 19385620, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 19385683 | HCID 19385683 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 19385620 | HCID 19385620 | 66.9% |
Reaction Steps
A solution of the product of Step B (26 mg, 0.096 mmol) NBS (16 mg, 0.95 eq) and AIBN (2 mg, catalytic amount) in CCl4 (2 mL) was heated to reflux for 1 hour and then concentrated in vacuo. The residue was purified on a silica gel flash chromatography column (125×20 mm) eluted with 5% ethyl acetate/hexane to yield 21 mg (62%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05449682 |
| Source dataset | uspto-grants-1995_09 |
| ORD ID | ord-ce4be18d8d0e4d068c94bc7b84389c25 |
| Source note | uspto-grants-1995_09 |