Methyl chloroformate → HCID 19385945, compound

HRID 2399533Notes

Reaction equation

HRID 2399533 reaction equation
[C:1](Cl)(=[O:4])[O:2][CH3:3].[CH3:6][C:7]1([CH3:30])[CH2:12][CH:11]([NH:13][CH2:14][CH2:15][CH2:16][NH:17][CH:18]2[CH2:23][C:22]([CH3:25])([CH3:24])[NH:21][C:20]([CH3:27])([CH3:26])[CH2:19]2)[CH2:10][C:9]([CH3:29])([CH3:28])[NH:8]1>O>[CH3:3][O:2][C:1]([N:13]([CH:11]1[CH2:12][C:7]([CH3:30])([CH3:6])[NH:8][C:9]([CH3:29])([CH3:28])[CH2:10]1)[CH2:14][CH2:15][CH2:16][N:17]([C:1]([O:2][CH3:3])=[O:4])[CH:18]1[CH2:19][C:20]([CH3:27])([CH3:26])[NH:21][C:22]([CH3:25])([CH3:24])[CH2:23]1)=[O:4]

Participants

4

Reactant 2

HCID 6586Methyl chloroformateHCID 19031689N~1~,N~3~-Bis(2,2,6,6-tetramethylpiperidin-4-yl)propane-1,3-diamine

Product 1

HCID 19385945HCID 19385945, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

83.2 g (0.88 mol) of methyl chlorocarbonate are reacted as described in Example 1 with 141 g (0.4 mol) of N,N'-bis(2,2,6,6-tetramethyl-4-piperidyl)-1,3-propanediamine dissolved in 420 ml of water.

Sources & evidence

ORD record
ord-9589eee79f1a4aa5adeff127a461883b
Source dataset
uspto-grants-1995_09
Patent number
US05449779

Reaction notes

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