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HRID2399958

反应详情

EQUATION

反应方程式

HRID 2399958 的结构方程式

REACTANTS

反应物

2
结构：CCO
HCID702

Ethanol

C2H6O

结构：COc1cc(C(=O)N(C(C)C)C(C)C)ccc1OCCCCCOc1ccc(C=NN)cc1.Cl
HCID67744755

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc(C(=O)N(C(C)C)C(C)C)ccc1OCCCCCOc1ccc(C=NN)cc1
HCID183800

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

Amberlite IRA-400 (OH) ion-exchange resin (55.5 g) is added in one portion to a stirred ethanol (120 mL)/methanol (30 mL) solution of 4-[5-[4-(aminoiminomethyl)phenoxy] pentyloxy]-3-methoxy-N,N-bis(1-methylethyl)benzamide monohydrochloride (20 g). After stirring for 20 hours, the resin is removed by filtration. The mother liquor is concentrated at reduced pressure to afford 4-[5-[4-(aminoiminomethyl)phenoxy]pentyloxy]-3-methoxy-N,N-bis(1-methylethyl)benzamide.

WORKUP

后处理

  1. customthe resin is removed by filtration
  2. concentrationThe mother liquor is concentrated at reduced pressure