Tert-butylcarbamate → HCID 19382370, compound

HRID 2400049Notes

Reaction equation

C([NH:5][C:6](=O)[O-:7])(C)(C)C.[C:9]([C:17]1OC=[CH:20][C:21]=1NC(=O)OC(C)(C)C)(=[O:16])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>>[NH2:5][C:6]1[O:7][CH:20]=[CH:21][C:17]=1[C:9](=[O:16])[C:10]1[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=1

Participants

Reactant 2

HCID 21252905Tert-butylcarbamate

HCID 54179133HCID 54179133, compound

Product 1

HCID 19382370HCID 19382370, compound

Procedure

Hydrolysis of the t-butylcarbamate according to the procedure for compounds 5 and 6 in which compound 28 is substituted for compound 4 gives the 2-amino-3-benzoylfuran, compound 29.

Sources & evidence

ORD record: ord-f46b3e061cb34587bfaaedd79cb8a2e3
Source dataset: uspto-grants-1995_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05453424

Reaction notes

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