HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → HCID 19382186, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | Ethyl 1-oxa-6-azaspiro[2,5]octane-6-carboxylate | HCID 13672926 | — |
| Product | HCID 19382186 | HCID 19382186 | — |
Reaction Steps
5.7 g (30.8 mmol) of ethyl 6-aza-1-oxaspiro[2,5]octane-6-carboxylate are added dropwise to 30 ml of ethylamine solution (50% in water) and the mixture is stirred overnight at room temperature. It is then concentrated and distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05453422 |
| Source dataset | uspto-grants-1995_09 |
| ORD ID | ord-316e70911c3348dbab823113457d1988 |
| Source note | uspto-grants-1995_09 |