HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19382746, compound → HCID 19382745, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19382746 | HCID 19382746 | — |
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 19382745 | HCID 19382745 | — |
Reaction Steps
0.7 ml of 4N-hydrochloric acid-1,4-dioxane solution were dropwise added to a solution of 484 mg of 4-acetyl-3,5-dimethyl-1H-pyrazole-1-carboxamidine in 1 ml of ethanol and 5 ml of ether. The crystals precipitated out were taken out by filtration to obtain 488 mg of 4-acetyl-3,5-dimethyl-1H-pyrazole-1-carboxamidine hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05453514 |
| Source dataset | uspto-grants-1995_09 |
| ORD ID | ord-54966feb0a1640029071a2fa2df6347b |
| Source note | uspto-grants-1995_09 |