Sodium borohydride → HCID 53993586, compound

Participants

Reaction Steps

The product from Step 5 of Example 7 (150 mg) was dissolved in 20 mL of MeOH, and treated with 15 mg of NaBH4 at 0° C. After 10 min. the mixture was quenched with 10 mL of sat. NH4Cl, and extracted with 50 mL of EtOAc. The extract was dried over NaSO4 and concentrated to give 150 mg of the title compound.

Provenance & Evidence