HCID 86694066, compound → HCID 86694067, compound

Participants

Reaction Steps

A mixture of (2S,5R)-6-(benzyloxy)-7-oxo-N′-(pyridin-3-yl)-1,6-diazabicyclo[3.2.1]octane-2-carbohydrazide 238 (0.20 g, 0.54 mmol) and Pd/C (0.08 g) in methanol (20 mL) was hydrogenated at 1 atm at room temperature for 3 h. The mixture was filtered through Celite pad and concentrated to provide 239 (0.13 g, 87%) as a white foam.

Provenance & Evidence