HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 86666721, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | HCID 67814319 | HCID 67814319 | — |
| Reactant | HCID 86666719 | HCID 86666719 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86666721 | HCID 86666721 | — |
Reaction Steps
A procedure similar to the synthesis of (2-(3-(1-azidoethyl)-5-methylisoxazol-4-yl)phenyl)(4-chlorophenyl)methanone in Example 16 was followed, except that DMF was substituted by a mixture of acetonitrile and water; and that (4-Chlorophenyl)(2-fluoro-4-(5-(hydroxymethyl)-3-methylisoxazol-4-yl)pyridin-3-yl)methanone was used as starting material. LC/MS m/z 372 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08796261B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-fd49a5b33e514580944b63023d312a3f |
| Source note | uspto-grants-2014_08 |