Pyridine → HCID 11346227, compound

HRID 2401965Notes

Reaction equation

HRID 2401965 reaction equation
Cl[C:2]1[C:10]2[C:6](=[N:7][O:8][N:9]=2)[C:5]([N+:11]([O-:13])=[O:12])=[CH:4][CH:3]=1.[SH:14][CH2:15][CH2:16][C:17]([OH:19])=[O:18].N1C=CC=CC=1>C(O)C.O>[N+:11]([C:5]1[C:6]2=[N:7][O:8][N:9]=[C:10]2[C:2]([S:14][CH2:15][CH2:16][C:17]([OH:19])=[O:18])=[CH:3][CH:4]=1)([O-:13])=[O:12]

Participants

5

Reactant 3

HCID 1049PyridineHCID 65143-Mercaptopropionic AcidHCID 25043NBD-Cl

Product 1

HCID 11346227HCID 11346227, compound

Reagents, catalysts & solvents 1

HCID 19096565Water ethanolSolvent

Procedure

A solution of 4-chloro-7-nitro-2,1,3-benzoxadiazole (1 mmole) and 3-mercaptopropionic acid (Sigma-Aldrich, Fine Chemicals) (1 mmole) was made to react in 6 ml of ethyl alcohol: water 0.3:1 containing 2.5 mmoles of pyridine.

Sources & evidence

ORD record
ord-4fce225879734898a04ac6e899023f44
Source dataset
uspto-grants-2014_08
Patent number
US08796317B2

Reaction notes

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