Diethyl Ether → HCID 67199887, compound

Participants

Reaction Steps

N,N-dimethyl-4-(pyridine-4-yl)aniline (0.1 g, 5.5 mmols) was dissolved in acetonitrile (50 ml) and ethyl iodide (4 ml) was added. The mixture was heated at reflux for 4 hours then cooled to ambient temperature. Diethylether (50 ml) was added IDT321 (0.035 g, 0.9 mmols) crystallized upon standing and was removed via filtration. 1H NMR (DMSO-d6) δ 1.50 (t, 3H), 3.40 (s, 6H), 4.50 (q, 2H), 6.95 (d, 2H), 8.05 (d, 2H), 8.35 (d, 2H), 8.90 (d, 2H).

Provenance & Evidence