HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 67199580, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Pyridine, 4-(4-dimethylaminophenyl)- | HCID 227783 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 67199580 | HCID 67199580 | 29% |
Reaction Steps
Was prepared by refluxing N,N-dimethyl-4-(pyridine-4-yl)aniline (II) in acetonitrile in the presence of ethyl iodide. After which the solution was cooled to room temperature. Ether was added and the product crystallized resulting in a 29% of 4-(4-(dimethylamino)phenyl)-1-propylpyridinium iodide (IDT322) (V).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08647827B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-b07a24d5d5db4c96befcd6e4ddf206b3 |
| Source note | uspto-grants-2014_02 |