Naptalam → HCID 131731191, compound

HRID 240237Notes

Reaction equation

HRID 240237 reaction equation
C1C(C2C3C(=CC=CC=3)C=CC=2)C(=O)O/C(=C/Br)/C1.[CH:20]1[C:25]([Cl:26])=[CH:24][C:23]([Cl:27])=[C:22]([O:28][CH2:29][C:30]([OH:32])=[O:31])[CH:21]=1.[CH:33]1[CH:34]=[C:35]([N:40]2[CH2:45][CH2:44][NH:43][CH2:42][CH2:41]2)[CH:36]=[C:37]([Cl:39])[CH:38]=1.[CH3:46][O:47][C:48]1[C:49]([Cl:58])=[CH:50][CH:51]=[C:52]([Cl:57])[C:53]=1[C:54]([OH:56])=[O:55].[CH:59]1[CH:60]=[CH:61][C:62]2[C:63](=[CH:65][CH:66]=[CH:67][C:68]=2[NH:69][C:70]([C:72]2[CH:73]=[CH:74][CH:75]=[CH:76][C:77]=2[C:78]([OH:80])=[O:79])=[O:71])[CH:64]=1>>[CH:20]1[C:25]([Cl:26])=[CH:24][C:23]([Cl:27])=[C:22]([O:28][CH2:29][C:30]([OH:32])=[O:31])[CH:21]=1.[CH:33]1[CH:34]=[C:35]([N:40]2[CH2:45][CH2:44][NH:43][CH2:42][CH2:41]2)[CH:36]=[C:37]([Cl:39])[CH:38]=1.[CH3:46][O:47][C:48]1[C:49]([Cl:58])=[CH:50][CH:51]=[C:52]([Cl:57])[C:53]=1[C:54]([OH:56])=[O:55].[CH:59]1[CH:60]=[CH:61][C:62]2[C:63](=[CH:65][CH:66]=[CH:67][C:68]=2[NH:69][C:70]([C:72]2[CH:73]=[CH:74][CH:75]=[CH:76][C:77]=2[C:78]([OH:80])=[O:79])=[O:71])[CH:64]=1

Participants

4

Reactant 3

HCID 8594Naptalam2×HCID 59402646-(Bromomethylene)tetrahydro-3-(1-naphthaleneyl)-2H-pyran-2-oneHCID 131731192HCID 131731192, compound2×

Product 1

HCID 131731191HCID 131731191, compound

Procedure

Seedlings of sunflower (helianthus sp. HELSS) were treated with postemergence applications of either a mixture of 2,4-D+MCPP+dicamba at 208+56+22 g ae/ha or at 83+22+9 g ae/ha, or naptalam at 56 g ae/ha, or the combination of 2,4-D+MCPP+dicamba and naptalam at 208+56+22+56 g ae/ha or at 83+22+9 g+56 g ae/ha, respectively, when they were 8-10 cm in height. All treatment mixtures contained 0.25% (v/v) non-ionic surfactant. Plants were placed in a completely randomized design with four replications per treatment. Percent injury data was collected 10 days after treatment (DAT). The results are summarized in table 7.

Workup

  1. customPercent injury data was collected 10 days after treatment (DAT)

Sources & evidence

ORD record
ord-0b191577ade04a40ba4af94577dbe439
Source dataset
uspto-grants-2014_02
Patent number
US08648012B2

Reaction notes

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