Methacrylic Acid → HCID 89106266, compound

HRID 2402484Notes

Reaction equation

HRID 2402484 reaction equation
FF.[C:3]([OH:8])(=[O:7])[C:4]([CH3:6])=[CH2:5].[F:9][C:10](=[C:15]([F:17])[F:16])[CH2:11][CH2:12][CH2:13]O>>[C:3]([O:8][CH2:13][CH2:12][CH2:11][C:10]([F:9])=[C:15]([F:17])[F:16])(=[O:7])[C:4]([CH3:6])=[CH2:5]

Participants

4

Reactant 3

HCID 4093Methacrylic AcidHCID 24524Fluorine2×HCID 27779334,5,5-Trifluoro-4-penten-1-ol

Product 1

HCID 89106266HCID 89106266, compoundYield 43%

Procedure

A fluorine based polymer was also tested to provide a plasma reactive functionality. The fluorine based monomer used to form the polymer was synthesized by the reaction of methacrylic acid and 4,5,5-trifluoropent-4-en-1-ol to yield 4,5,5-trifluoropent-4-enyl methacrylate. This yield was about 43%. The chemical structure of 4,5,5-trifluoropent-4-enyl methacrylate is shown in Formula (IV):

Workup

  1. customto provide a plasma reactive functionality
  2. customto form the polymer

Sources & evidence

ORD record
ord-850b813d61974f04954da01ebc16ae3f
Source dataset
uspto-grants-2014_08
Patent number
US08796372B2

Reaction notes

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