HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylaziridine → N,N'-1,6-Hexanediylbis(2-methyl-1-aziridinecarboxamide)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylaziridine | HCID 6377 | — |
| Reactant | Hexamethylene diisocyanate | HCID 13192 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N,N'-1,6-Hexanediylbis(2-methyl-1-aziridinecarboxamide) | HCID 97887 | — |
Reaction Steps
2-Methyl aziridine (15.05 grams, 0.26 moles) was added drop wise over one hour to a solution of 1,6-diisocyanatohexane (20.00 grams, 0.12 moles, Aldrich) in toluene (40 mL) while cooling in an ice bath. After stirring for a total of 24 hours at room temperature, a potion of the solvent was removed under vacuum to give N,N′-(hexane-1,6-diyl)bis-(2-methylaziridine-1-carboxamide)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08796390B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-f11258f252a5408ab43c6953d35ae18c |
| Source note | uspto-grants-2014_08 |