HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → 2-Bromo-1-(4-fluoro-3-methylphenyl)ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | 1-(4-Fluoro-3-methylphenyl)ethan-1-one | HCID 289328 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 2-Bromo-1-(4-fluoro-3-methylphenyl)ethanone | HCID 10977301 | — |
Reaction Steps
0.67 mL bromine was added to 2 g 1-(4-fluoro-3-methyl-phenyl)-ethanone in 10 mL conc. acetic acid. The reaction was stirred 3 h at RT. The mixture was added to ice water. The precipitate was filtered, washed with water and dried to give 2.7 g desired product. Rt: 1.10 min (method A), (M+H)+: 231
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08796467B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-b2bdef4bf7c54a74a6e3da2508fc951c |
| Source note | uspto-grants-2014_08 |