HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68646783, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 59536818 | HCID 59536818 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 68646783 | HCID 68646783 | — |
Reaction Steps
Of the compound from Example 186A, 345 mg (0.92 mmol) were admixed with 10 ml of a 4N solution of hydrogen chloride in dioxane, and the mixture was stirred at RT for 30 min All volatile constituents were then removed on a rotary evaporator. The residue (311 mg, 100% of theory) was the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08796324B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-48211adb30d7448aa731bfed82859289 |
| Source note | uspto-grants-2014_08 |