HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 89388365, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 89388363 | HCID 89388363 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 89388365 | HCID 89388365 | — |
Reaction Steps
A solution of Example 158B (200 mg, 0.4 mmol) in dichloromethane (10 ml) was treated with TFA (5 mL) at 40° C. overnight. The volatiles were removed and the residue was directly used in the next step without further purification. MS (DCI/NH3) m/z 474 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08796289B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-6f1bd9c1885b4d56891789825a26ae9d |
| Source note | uspto-grants-2014_08 |