HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2402957Generated: November 1, 2026
Trifluoroacetic acid → HCID 89388442, compound
https://huagongshe.com/reaction/2402957
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 89388346 | HCID 89388346 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 89388442 | HCID 89388442 | — |
Reaction Steps
To a solution of Example 215A (500 mg, 1.32 mmol) in dichloromethane (20 ml) was added TFA (5 mL). The mixture was stirred at 40° C. overnight. The reaction mixture was concentrated and the crude product was used in the next step without further purification. MS (DCI/NH3) m/z 331 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08796289B2 |
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| Source dataset | uspto-grants-2014_08 |
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| ORD ID | ord-04f173eef3bb4473a189f6494f0a4bb9 |
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| Source note | uspto-grants-2014_08 |
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