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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2402957Generated: November 1, 2026

Trifluoroacetic acid → HCID 89388442, compound

https://huagongshe.com/reaction/2402957

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 89388346HCID 89388346—
SolventDichloromethaneHCID 6344—
ProductHCID 89388442HCID 89388442—

Reaction Conditions

Temperature40 °C

Reaction Steps

To a solution of Example 215A (500 mg, 1.32 mmol) in dichloromethane (20 ml) was added TFA (5 mL). The mixture was stirred at 40° C. overnight. The reaction mixture was concentrated and the crude product was used in the next step without further purification. MS (DCI/NH3) m/z 331 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08796289B2
Source datasetuspto-grants-2014_08
ORD IDord-04f173eef3bb4473a189f6494f0a4bb9
Source noteuspto-grants-2014_08