Didecyldimethylammonium → HCID 178443399, compound

HRID 2403124Notes

Reaction equation

HRID 2403124 reaction equation
[CH2:1]([N+:11]([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23])([CH3:13])[CH3:12])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[C:24]([O-:33])(=[O:32])[C:25]1[C:26](=[CH:28][CH:29]=[CH:30][CH:31]=1)[OH:27].[Na+]>O>[C:24]([O-:33])(=[O:32])[C:25]1[C:26](=[CH:28][CH:29]=[CH:30][CH:31]=1)[OH:27].[CH2:14]([N+:11]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10])([CH3:13])[CH3:12])[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23]

Participants

4

Reactant 2

HCID 16958DidecyldimethylammoniumHCID 16760658Sodium Salicylate

Product 1

HCID 178443399HCID 178443399, compoundYield 90%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
60 °C

Procedure

The stechiometric amounts of didecyldimethylammonium saccharinate and sodium salicylate were mixed in distilled water and stirred at 60° C. for 2 h. After that time the solution was cooled to room temperature. The product was extracted from the aqueous solution with chloroform. The chloroform phase was removed and solvent was evaporated. Synthesized didecyldimethylammonium salicylate (90% yield) was dried under vacuum.

Workup

  1. temperatureAfter that time the solution was cooled to room temperature
  2. extractionThe product was extracted from the aqueous solution with chloroform
  3. customThe chloroform phase was removed
  4. customsolvent was evaporated

Sources & evidence

ORD record
ord-c71caa8ec404435bae3bf2b759ef8154
Source dataset
uspto-grants-2014_08
Patent number
US08802596B2

Reaction notes

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