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HRID2403158

反应详情

EQUATION

反应方程式

HRID 2403158 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)C(Br)CCBr
HCID296716

Methyl 2,4-dibromobutanoate

C5H8Br2O2

结构：CC1(C)CCC(N)CC1.Cl
HCID24191928

4,4-Dimethylcyclohexan-1-amine--hydrogen chloride (1/1)

C8H18ClN

PRODUCTS

生成物

1
结构：COC(=O)C1CCN1C1CCC(C)(C)CC1
HCID86692751

未命名化合物

收率 52%

PROCEDURE

实验过程

The reaction of methyl 2,4-dibromobutanoate 17 with 4,4-dimethylcyclohexylamine hydrochloride 18C yielded methyl 1-(4,4-dimethylcyclohexyl)azetidine-2-carboxylate as a brown oil (52%). MS ISP (m/e): 226.3 (100) [(M+H)]+.