Hydrochloric Acid → HCID 76577938, compound

Participants

Reaction Steps

To a solution of 37 (70 mg, 0.2 mmol) in THF/H2O (1:1, 15 ml) LiOH.H2O (41 mg, 1.0 mmol) was added and the mixture was stirred at room temperature. After 2 h 2N HCl was added up to pH=5. The solvent was removed under reduced pressure and the crude was purified by flash chromatography (CH2Cl2/MeOH/AcOH 90:10:1) affording 38 (41 mg, 63%) as yellow solid. ESI+MS: calcd for C15H9N5O4: 323.27; found: 324.3 (MH+).

Provenance & Evidence