HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → 4-Methoxybenzyl bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 4-Methoxybenzyl alcohol | HCID 7738 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 4-Methoxybenzyl bromide | HCID 165021 | — |
Reaction Steps
A solution of 4-methoxybenzylalcohol (10 g) in ether (300 ml) was shaken with hydrobromic acid, 48%, (150 ml). The organic phase was washed with saturated sodium bromide, dried (K2CO3) and the solvents removed in vacuo to give 4-methoxybenzylbromide (13.17 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08802670B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-188f3c8abff24bb9895af629aa8ecf5e |
| Source note | uspto-grants-2014_08 |