Sarcosine t-butyl ester hydrochloride → HCID 66677563, compound

HRID 2404340Notes

Reaction equation

HRID 2404340 reaction equation
Br[CH2:2][C:3]1[CH:4]=[C:5]([CH:8]=[CH:9][C:10]=1[Cl:11])[C:6]#[N:7].Cl.[C:13]([O:17][C:18](=[O:22])[CH2:19][NH:20][CH3:21])([CH3:16])([CH3:15])[CH3:14]>>[Cl:11][C:10]1[CH:9]=[CH:8][C:5]([C:6]#[N:7])=[CH:4][C:3]=1[CH2:2][N:20]([CH3:21])[CH2:19][C:18]([O:17][C:13]([CH3:16])([CH3:15])[CH3:14])=[O:22]

Participants

3

Reactant 2

HCID 11252350Sarcosine t-butyl ester hydrochlorideHCID 666777673-(Bromomethyl)-4-chlorobenzonitrile

Product 1

HCID 66677563HCID 66677563, compound

Procedure

The title compound was prepared following general procedure 10, starting from 3-(bromomethyl)-4-chlorobenzonitrile and sarcosine tert-butyl ester hydrochloride. It was obtained as a colorless oil (1.9 g, 86%). LC/MS (Method B): 295.1 (M+H)+.

Sources & evidence

ORD record
ord-02cde4600ac946c691d8651f5c5ff806
Source dataset
uspto-grants-2014_08
Patent number
US08802704B2

Reaction notes

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