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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2404410Generated: November 3, 2026

HCID 49963717, compound → HCID 66836093, compound

https://huagongshe.com/reaction/2404410

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 49963717HCID 49963717—
CatalystManganeseHCID 23930—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 66836093HCID 66836093—

Reaction Steps

To a solution of (benzothiazol-2-yl)(m-tolyl)methanol (2.41 g) in dioxane (30 mL) is added manganese dioxyde (1.2 molar equivalent). The mixture is stirred overnight at room temperature, then filtered over a clarcel pad. The filtrate is concentrated under reduced pressure. The residue is triturated in heptane and diisopropyl oxyde to give (benzothiazol-2-yl)(m-tolyl)methanone

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08802664B2
Source datasetuspto-grants-2014_08
ORD IDord-11fafcb8bfd946ee949f052405972343
Source noteuspto-grants-2014_08