HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 49963717, compound → HCID 66836093, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 49963717 | HCID 49963717 | — |
| Catalyst | Manganese | HCID 23930 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 66836093 | HCID 66836093 | — |
Reaction Steps
To a solution of (benzothiazol-2-yl)(m-tolyl)methanol (2.41 g) in dioxane (30 mL) is added manganese dioxyde (1.2 molar equivalent). The mixture is stirred overnight at room temperature, then filtered over a clarcel pad. The filtrate is concentrated under reduced pressure. The residue is triturated in heptane and diisopropyl oxyde to give (benzothiazol-2-yl)(m-tolyl)methanone
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08802664B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-11fafcb8bfd946ee949f052405972343 |
| Source note | uspto-grants-2014_08 |