HCID 60151763, compound → HCID 60151906, compound

Participants

Reaction Conditions

Reaction Steps

Add Pd/C (80 mg) to a solution of 3-(4-dimethylaminomethyl-bicyclo[3.2.1]oct-2-en-3-yl)-phenol (250 mg, 0.97 mmol) in MeOH (40 mL). Then stir the mixture at 25° C. for 12 hours under 45 PSI of H2. After filtration, Concentrate the solution under vacuum to afford 3-(2-dimethylaminomethyl-bicyclo[3.2.1]oct-3-yl)-phenol as white solid (252 mg, Yield: 100%). MS (m/z): 260 (M+1).

Provenance & Evidence